Calibration-free laser-induced plasma spectrometry for direct analysis of solid and liquid materials

Michail V. Belkov; Victor S. Burakov; Vasilii V. Kiris; Sergei N. Raikov

doi:10.1117/12.752971

9 July 2007 Calibration-free laser-induced plasma spectrometry for direct analysis of solid and liquid materials

Michail V. Belkov, Victor S. Burakov, Vasilii V. Kiris, Sergei N. Raikov

Proceedings Volume 6733, International Conference on Lasers, Applications, and Technologies 2007: Environmental Monitoring and Ecological Applications; Optical Sensors in Biological, Chemical, and Engineering Technologies; and Femtosecond Laser Pulse Filamentation; 673307 (2007) https://doi.org/10.1117/12.752971
Event: International Conference on Lasers, Applications, and Technologies '07, 2007, Minsk, Belarus

Abstract

Optical diagnostics of laser ablation plasma has provided the opportunity to realize calibration-free analyses of solid and liquid materials. In general, this variant of optical emission spectroscopy of pulsed plasma allows the matrix effects to be overcome, yielding satisfactorily precise and accurate quantitative results on elemental composition of materials without using calibration curves, certified reference materials, and internal standards. Such analysis for solids is very close to be nondestructive due to the minimum possible ablated mass, a feature which is very important in many applications, especially for unique museum exhibits and jeweler samples. In this paper, the use of the method for the analysis of elements mainly in metallic alloys, glass samples, and archaeological findings is demonstrated. The results presented confirm the suitability of the approach for routine applications of our instrumentation, while at the same time simplifying the overall analytical procedure.

Citation Download Citation

Michail V. Belkov, Victor S. Burakov, Vasilii V. Kiris, and Sergei N. Raikov "Calibration-free laser-induced plasma spectrometry for direct analysis of solid and liquid materials", Proc. SPIE 6733, International Conference on Lasers, Applications, and Technologies 2007: Environmental Monitoring and Ecological Applications; Optical Sensors in Biological, Chemical, and Engineering Technologies; and Femtosecond Laser Pulse Filamentation, 673307 (9 July 2007); https://doi.org/10.1117/12.752971

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